HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 21459557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 12040166 | HCID 12040166 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 21459557 | HCID 21459557 | — |
Reaction Steps
3,4,5-Tribromo-pyrrole-2-carbonitrile (1.0 g, 0.003 mol) is dissolved in a mixture of acetone (20 mL) and dimethoxyethane (10 mL). potassium carbonate (0.45 g, 0.0033 mol) is added followed by methyl iodide (0.478 g, 0.0033 mol). After stirring overnight at room temperature, the mixture is poured into water precipitating a white solid. The solid (0.8 g, 80%) has mp 115°-119° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05702681 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-a6934eb800444331ac906af2975df62a |
| Source note | uspto-grants-1997_12 |