HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 18925574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 21459573 | HCID 21459573 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18925574 | HCID 18925574 | — |
Reaction Steps
2.52 g (6.44 mmol) of the ester obtained in Example 8, in solution in 30 ml of methanol, were treated with 2.5 g of sodium hydroxide and heated at reflux for 3 hours. After the same treatment as in Example 7, followed by recrystallization from hexane, 2.35 g (97%) of the expected coompound, melting at 262°-264° C., are isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05702710 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-4c3bf28ed02a4cb4b2697217059896c3 |
| Source note | uspto-grants-1997_12 |