HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 178506034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Propane, 1-bromo-3-fluoro- | HCID 67699 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178506034 | HCID 178506034 | 85.2% |
Reaction Steps
3-Fluorobromopropane (200.0 g, 1.42 mol) was dissolved in toluene (3), followed by adding to the solution, triphenylphosphine (37.2 g, 1.42 mol), refluxing the mixture for 15 hours, filtering off the resulting product, and suction-drying, to obtain 3-fluoropropyltriphenylphosphine bromide (486 g, 1.21 mol). Yield: 85.2%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05702641 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-e4e6cd7fe3bc460b9acc0cf9d888fa4a |
| Source note | uspto-grants-1997_12 |