Phosphorus oxychloride → 12-Chlorobenz[b]acridine

HRID 1941076Notes

Reaction equation

HRID 1941076 reaction equation
[NH:1]([C:8]1[C:9]([C:18](O)=O)=[CH:10][C:11]2[C:16]([CH:17]=1)=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.P(Cl)(Cl)([Cl:23])=O>>[Cl:23][C:18]1[C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[N:1]=[C:8]2[C:9]=1[CH:10]=[C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:16]1=[CH:17]2

Participants

3

Reactant 2

HCID 24813Phosphorus oxychlorideHCID 1388882-Naphthalenecarboxylic acid, 3-(phenylamino)-

Product 1

HCID 1476981312-Chlorobenz[b]acridine

Procedure

treating 3-anilino-2-naphthoic acid with phosphorous oxychloride to produce 12-chloro-benz[b]acridine;

Sources & evidence

ORD record
ord-b1eda5e72d1d4973bf66c61987c9208c
Source dataset
uspto-grants-1997_12
Patent number
US05702887

Reaction notes

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