HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86751772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86751771 | HCID 86751771 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86751772 | HCID 86751772 | — |
Reaction Steps
2.78 g (5.74 mmol) of ethyl (3-(4-(tert-butyloxycarbonylaminoiminomethyl)benzyl)-3-benzyloxyureido)acetate in 50 ml of ethanol are treated with 0.23 g (5.74 mmol) of NaOH and 1.2 ml of water and the mixture is stirred at room temperature for 18 h. The solvent is removed in vacuo and the residue is freeze-dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703050 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-cebfd883ae3f457792f9835f1f4d554b |
| Source note | uspto-grants-1997_12 |