HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22880589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22880591 | HCID 22880591 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22880589 | HCID 22880589 | 70% |
Reaction Steps
Methyl 2(R)-(N-butyloxycarbonylamino)-4-(p-toluenesulfonylamino)butyrate (2.0 g, 5.18 mmol) was dissolved in 10 mL 4N HCl in dioxane and the solution was stirred for 1 hour and then concentrated. The residue was triturated with ether to give 1.16 g (70%) product. ES-MS: calcd M+1 287.2; found 287.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703092 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-7bd5d083cc3e4c808c04201d766c4ce8 |
| Source note | uspto-grants-1997_12 |