HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetaldehyde → HCID 12385029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetaldehyde | HCID 998 | — |
| Reactant | Dimethyl Sulfide | HCID 1068 | — |
| Product | HCID 12385029 | HCID 12385029 | 80% |
Reaction Steps
Using the method of Example 36 with phenylacetaldehyde but using (1 mmol) of dimethyl sulfide gave the title compound in 80% yield as a clear oil. δH (CDCl3, 250 MHz): 7.3-7.1 (10H,m), 3.55 (1H,d,J=2.0 Hz), 3.05 (1H, dt,J=6.0 Hz,J=2.0 Hz), 2.80 (2H,d,J=6.0 Hz)ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703246 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-f1f4dac020bc47ffbc0f4f6c65550c5b |
| Source note | uspto-grants-1997_12 |