HCID 22106551, compound → HCID 22106524, compound

Participants

Reaction Steps

A suspension of 1-(4-benzyloxy-3-fluoro-phenyl)-5-methyl-1H-tetrazole (4.6 g) in ethanol (300 ml) was hydrogenated at room temperature and pressure over a pre-reduced suspension of palladium-on-carbon (10% paste, 1.4 g) until uptake ceased. The catalyst was filtered off and the filtrate evaporated to give the title compound as a cream solid (3.6 g). T.l.c. (Dichloromethane/methanol (995:5)), Rf 0.45.

Provenance & Evidence