HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22106522, compound → HCID 22106583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22106522 | HCID 22106522 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22106583 | HCID 22106583 | 98.7% |
Reaction Steps
A solution of 1-(4-benzyloxy-phenyl)-5-cyclopropyl-1H-tetrazole (2.3 g) in ethanol (75 ml) was added to a suspension of 10% palladium on charcoal catalyst (400 mg) in ethanol (10 ml) and the mixture was stirred under a hydrogen atmosphere for 1 h. The catalyst was removed by filtration and the solution concentrated in vacuo to afford the title compound (1.57 g) as a pale yellow solid, m.p. 184°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703240 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-c7b854f9b4874d96acd430360a511ee6 |
| Source note | uspto-grants-1997_12 |