HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Formyl-4-methoxyphenyl)boronic acid → HCID 22106460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Formyl-4-methoxyphenyl)boronic acid | HCID 2759225 | — |
| Reactant | HCID 22106464 | HCID 22106464 | — |
| Reactant | HCID 22106481 | HCID 22106481 | — |
| Product | HCID 22106460 | HCID 22106460 | — |
Reaction Steps
From a mixture of 5-bromo-1-cyclopropylmethyl-1H-tetrazole with 5-bromo-2-cyclopropyl-2H-tetrazole (1.91 g) and 3-formyl-4-methoxy-phenyl-boronic acid (1.86 g) to give the title compound (657 mg) as a yellow solid. NMR (CDCl3) δ 0.45 (2H,m); 0.70 (2H,m); 1.3 (1H,m); 4.05 (3H,s); 4.3(2H,d); 7.2 (1H,d); 8.0 (1H,m); 8.15 (1H,d); 10.55 (1H,s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703240 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-373c9c3ea3b24c5194b229ecdab32287 |
| Source note | uspto-grants-1997_12 |