HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+)-Fucose → HCID 15559381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+)-Fucose | HCID 94270 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | HCID 15559381 | HCID 15559381 | — |
Reaction Steps
D-Fucose (6-deoxy D-galactose) was reduced [a composition in total of 500 ml containing D-fucose at 1% and 20 ml of the Raney-nickel catalyst] to produce D-fucitol (6-deoxy D-galactitol). FIG. 57(a) shows HPLC analysis results of D-fucose before reduction and FIG. 57(b) shows HPLC analysis results of 6-deoxy L-galactitol after the reduction. The optical rotation of 6-deoxy L-galactitol was +1.7, and FIG. 58 shows 13C NMR spectrum of 6-deoxy L-galactitol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08389248B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-5762e74bbce94cd5bdc2f97717ca399d |
| Source note | uspto-grants-2013_03 |