Potassium Nitrate → HCID 58346346, compound

Participants

Reaction Conditions

Reaction Steps

A solution of 8 (7.5 g, 25.4 mmol) in concentrated H2SO4 (30 mL) was treated portionwise at 0° C. with solid KNO3 (3.9 g, 38.6 mmol). After stirring at 0° C. for 2 h, the reaction mixture was poured into 500 mL of ice-water and the resulting precipitate was removed by filtration and washed with ice-cold water. The resulting solid was dried to yield 9 as a yellow solid (7.6 g, 87% yield).

Provenance & Evidence