HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 1,4-Dioxaspiro[4.5]decan-8-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-n-Propylamino-cyclohexanone-ethyleneketal | HCID 11820081 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1,4-Dioxaspiro[4.5]decan-8-amine | HCID 14634315 | — |
Reaction Steps
1,4-Dioxa-spiro[4.5]dec-8-ylamine (2A) is synthesized as been described for 1A using methanol which has been saturated with ammonia.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08389555B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-e8687a5ae88246758ffc64d836b635a3 |
| Source note | uspto-grants-2013_03 |