Acetic Acid → HCID 87210797, compound

Participants

Reaction Steps

1.94 g (6 mmol) N-(4,4-diethoxybutyl)adamantylcarboxamide, 7.5 mL of acetic acid, 3.75 mL of 1N aqueous hydrochloric acid and 30 mL ethanol are put together and stirred for 16 hours under argon atmosphere. Ethanol is evaporated. Then the resulting residue is dispersed in dichloromethane and extracted with saturated sodium bicarbonate solution. The organic phase is dried with sodium sulfate and the solvent evaporated in vacuum.

Provenance & Evidence