HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22116092, compound → HCID 58249669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22116092 | HCID 22116092 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58249669 | HCID 58249669 | 84% |
Reaction Steps
1-(tert-Butoxycarbonyl)-4-phenyl-1,2,5,6-tetrahydropyridin-3-carboxylic acid (5.63 g) was dissolved in methanol (60 ml), and thereto was added palladium-carbon (4.06 g), and the mixture was stirred under hydrogen atmosphere for 2 hours. The reaction solution was filtered on celite, and concentrated under reduced pressure to give the title compound (4.76 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08389511B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-749f8d62bca74c88a13bd610b23eea9e |
| Source note | uspto-grants-2013_03 |