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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1942516Generated: November 1, 2026

HCID 22116092, compound → HCID 58249669, compound

https://huagongshe.com/reaction/1942516

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22116092HCID 22116092—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 58249669HCID 5824966984%

Reaction Steps

1-(tert-Butoxycarbonyl)-4-phenyl-1,2,5,6-tetrahydropyridin-3-carboxylic acid (5.63 g) was dissolved in methanol (60 ml), and thereto was added palladium-carbon (4.06 g), and the mixture was stirred under hydrogen atmosphere for 2 hours. The reaction solution was filtered on celite, and concentrated under reduced pressure to give the title compound (4.76 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08389511B2
Source datasetuspto-grants-2013_03
ORD IDord-749f8d62bca74c88a13bd610b23eea9e
Source noteuspto-grants-2013_03