HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-N-methylbenzenamine → HCID 45139098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-N-methylbenzenamine | HCID 70272 | — |
| Reactant | HCID 86640785 | HCID 86640785 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 45139098 | HCID 45139098 | 27% |
Reaction Steps
This compound was prepared from (4-chloro-6-isopropoxy-[1,3,5]triazin-2-yl)-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-amine and 4-chloro-N-methyl aniline in analogy to example 1c. Chromatography on Si—NH2 gel (Isolute) using ethyl acetate as an eluent gave the title compound as a colorless solid in 27% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08389717B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-99cdf4addcc14fdbbb335c8b20ff8796 |
| Source note | uspto-grants-2013_03 |