HCID 46872055, compound → HCID 46872057, compound

Participants

Reaction Steps

4-(4-Pentafluoroethoxyphenylazo)aniline 1H NMR (300 MHz, CDCl3) δ7.89-7.79 (m, 4H), 7.32 (d, J=8.5 Hz, 2H), 6.73-6.76 (m, 2H), 4.09 (br s, 2H); ESIMS m/z 332 ([M+H]+). Step 2. Compound 22. 1H NMR (300 MHz, CDCl3) δ 7.96-7.92 (m, 4H), 7.60-7.57 (m, 2H), 7.38-7.35 (m, 2H), 6.86 (s, 1H), 6.26 (s, 1H), 3.75-3.45 (m, 11H), 3.22 (t, J=9.3 Hz, 1H), 1.33-1.26 (m, 6H); ESIMS m/z 578 ([M+H]+).

Provenance & Evidence