HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dihydro-1H-pyrido[3,4-b][1,4]oxazine → HCID 44610275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dihydro-1H-pyrido[3,4-b][1,4]oxazine | HCID 21961536 | — |
| Reactant | 3,5-Dibromo-4-methoxybenzoyl chloride | HCID 33779630 | — |
| Product | HCID 44610275 | HCID 44610275 | — |
Reaction Steps
By the same method as in the step d) of Example 2, 2,3-dihydro-1H-pyrido[3,4-b][1,4]-oxazine (180 mg, 0.587 mmol) and 3,5-dibromo-4-methoxy-benzoyl chloride (193 mg, 0.587 mmol) were reacted to obtain the target compound 5, (3,5-dibromo-4-methoxy-phenyl)-(2,3-dihydro-pyrido[3,4-b][1,4]oxazin-1-yl)-methanone, as white solid (85 mg, 34%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394792B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-719ba20ef2304f3b8e9e7bd9e1b6ed85 |
| Source note | uspto-grants-2013_03 |