HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dihydro-2,2-dimethyl-2H-pyrido[4,3-b]-1,4-oxazine → HCID 66936725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dihydro-2,2-dimethyl-2H-pyrido[4,3-b]-1,4-oxazine | HCID 15857210 | — |
| Reactant | 3,5-Dibromo-4-methoxybenzoyl chloride | HCID 33779630 | — |
| Product | HCID 66936725 | HCID 66936725 | 44.5% |
Reaction Steps
By the same method as in the step d) of Example 2, 2,2-dimethyl-3,4-dihydro-2H-pyrido[4,3-b][1,4]oxazine (60 mg, 0.36 mmol) was reacted with 3,5-dibromo-4-methoxy-benzoyl chloride (120 mg, 0.36 mmol) to obtain the target compound, (3,5-dibromo-4-methoxy-phenyl)-(2,2-dimethyl-2,3-dihydro-pyrido[4,3-b][1,4]oxazin-4-yl)-methanone (73 mg, 44%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394792B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-352561afba39490d901ea3800ba77857 |
| Source note | uspto-grants-2013_03 |