Piperazine → HCID 44608383, compound

Participants

Reaction Steps

By the same method as in Example 39, (3,5-dichloro-4-methoxy-phenyl)-(2,3-dihydro-pyrido[3,4-b][1,4]oxazin-1-yl)-methanone (100 mg, 0.29 mmol), lithium chloride (124 mg, 2.9 mmol) and piperazine (38 mg, 0.44 mmol) were reacted. The resulting solid was purified by recrystallizing from methanol to obtain the target compound 41 as pale-brown solid (40 mg, 47%).

Provenance & Evidence