Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1943711Generated: November 3, 2026

HCID 178526762, compound → HCID 178507989, compound

https://huagongshe.com/reaction/1943711

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178526762HCID 178526762—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 178507989HCID 178507989105.7%

Reaction Steps

In a 100 ml flask, 3-nitro-quinolin-4-ol (500 mg, 2.629 mmol) was dissolved in methanol (50 ml) and 10% palladium on active carbon (1.2 g, 10 w/w %) was added thereto and then stirred for 3 hours at room temperature under hydrogen atmosphere. The reaction mixture was filtered on celite and then evaporated under reduced pressure to obtain brown liquid (445 mg, quantitative yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08394792B2
Source datasetuspto-grants-2013_03
ORD IDord-d17fb2e84280475e91c8551abfda31fe
Source noteuspto-grants-2013_03