HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178526762, compound → HCID 178507989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178526762 | HCID 178526762 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178507989 | HCID 178507989 | 105.7% |
Reaction Steps
In a 100 ml flask, 3-nitro-quinolin-4-ol (500 mg, 2.629 mmol) was dissolved in methanol (50 ml) and 10% palladium on active carbon (1.2 g, 10 w/w %) was added thereto and then stirred for 3 hours at room temperature under hydrogen atmosphere. The reaction mixture was filtered on celite and then evaporated under reduced pressure to obtain brown liquid (445 mg, quantitative yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394792B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-d17fb2e84280475e91c8551abfda31fe |
| Source note | uspto-grants-2013_03 |