HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclobutanecarbonyl chloride → HCID 66925793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclobutanecarbonyl chloride | HCID 78705 | — |
| Reactant | (3R)-3-Aminopiperidine, 3-BOC protected | HCID 1514172 | — |
| Product | HCID 66925793 | HCID 66925793 | — |
Reaction Steps
Acylation of (R)-piperidin-3-yl-carbamic acid tert-butyl ester (300 mg) with cyclobutyl carbonylchloride (0.342 ml) was performed according to the method described for example 20c. The residue was concentrated in vacuo and used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394789B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-493d1c6d26e14848a45f4fd8bd63d86e |
| Source note | uspto-grants-2013_03 |