HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl bromide → HCID 66925877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 58147578 | HCID 58147578 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66925877 | HCID 66925877 | — |
Reaction Steps
Bromoacetyl bromide (0.137 ml) was added to a stirred solution of the product of example 95 (500 mg) and DIPEA (0.425 ml) in dichloromethane (20 ml) over a period of 6 h. The reaction mixture was concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394789B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-38997c412dae49d8a4191803f98bdd7b |
| Source note | uspto-grants-2013_03 |