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HRID1944181

反应详情

EQUATION

反应方程式

HRID 1944181 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：Cc1ccc(C(=O)OCc2ccc(C(CNC(=O)OC(C)(C)C)C(=O)Nc3ccc(C(N)=O)c(F)c3)cc2)c(C)c1
HCID59563699

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(C(=O)OCc2ccc(C(CN)C(=O)Nc3ccc(C(N)=O)c(F)c3)cc2)c(C)c1
HCID59563720

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

To 4-(3-(tert-butoxycarbonylamino)-1-(4-carbamoyl-3-fluorophenylamino)-1-oxopropan-2-yl)benzyl 2,4-dimethylbenzoate (E337-2) in CH2Cl2 was added HCl (4 N in dioxane) and the solution was stirred overnight. The solvents were evaporated to give pure 4-(3-amino-1-(4-carbamoyl-3-fluorophenylamino)-1-oxopropan-2-yl)benzyl 2,4-dimethylbenzoate (E338).

WORKUP

后处理

  1. customThe solvents were evaporated