Potassium Carbonate → HCID 63802187, compound

Participants

Reaction Steps

A mixture of 4-fluorobenzenethiol (0.93 g), potassium carbonate (3.1 g) and N,N-dimethylformamide (25 mL) was treated with 3,4-difluorobenzaldehyde (1.0 g), and the resulting mixture was stirred at room temperature for 16 hours. The mixture was partitioned between water and ethyl acetate, and the organic phase was dried over magnesium sulfate. The solvent was removed under reduced pressure to afford the title compound as a colourless gum (0.18 g).

Provenance & Evidence