HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1944392Generated: November 1, 2026
HCID 67044881, compound → HCID 86652183, compound
https://huagongshe.com/reaction/1944392
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 67044881 | HCID 67044881 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86652183 | HCID 86652183 | 66.2% |
Reaction Steps
A solution of N-(4-fluorophenyl)-2-hydroxymethyl-N-methylbenzenesulfonamide (0.35 g) in chloroform (20 mL) was treated with manganese dioxide (1.2 g), and the resulting mixture was stirred at 60° C. for 16 hours. The mixture was filtered through Celite and the filtrate concentrated under reduced pressure to afford the title compound as colourless oil (0.23 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08394836B2 |
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| Source dataset | uspto-grants-2013_03 |
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| ORD ID | ord-f5edb48802e94d7ebbac2029e66ee876 |
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| Source note | uspto-grants-2013_03 |
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