HRID19445

反应详情

EQUATION

反应方程式

HRID 19445 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

0.70 mol of N2,4-diphenylpyridine-2,3-diamine and 2.56 mol of ethoxymethylene malononitrile were added in 10 ml of isopropanol, and refluxed for 6 hours. The solution was removed and was purified by using column chromatography to thereby produce a solid crystalline product at a yield of 75%.

WORKUP

后处理

  1. temperaturerefluxed for 6 hours
  2. customThe solution was removed
  3. customwas purified
  4. customto thereby produce a solid crystalline product at a yield of 75%