HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-2-chlorobenzoic acid → HCID 86594440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-2-chlorobenzoic acid | HCID 17154 | — |
| Reactant | HCID 86594439 | HCID 86594439 | — |
| Product | HCID 86594440 | HCID 86594440 | 79% |
Reaction Steps
4-amino-2-chloro-benzoic acid was converted to product in 79% yield, using the procedure described for the synthesis of 4-tert-Butoxyamino-3-methyl-benzoic acid. 1H NMR (DMSO-d6): δ 1.49 (s, 9 H), 7.46 (d of d, 1 H), 7.71 (br s, 1 H), 7.80 (d, 1 H), 9.87 (s, 1 H) and 13.00 (br s, 1 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394828B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-b8b94d1023304f77ba3c492b5f4331e8 |
| Source note | uspto-grants-2013_03 |