HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazine → HCID 66815800, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazine | HCID 4837 | — |
| Reactant | HCID 18146450 | HCID 18146450 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 66815800 | HCID 66815800 | 202.4% |
Reaction Steps
A solution of 4-fluoro-N-quinolin-3-yl-benzamide (2.0 g, 3.76 mmol) and piperazine (6.2 g, 72 mmol) in methylsulfoxide (30 mL) was heated 100° C. for 1.5 days, to give the product 2.53 g (100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394828B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-a15389d660b848439029b184112863bc |
| Source note | uspto-grants-2013_03 |