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HRID1944574

反应详情

EQUATION

反应方程式

HRID 1944574 的结构方程式

REACTANTS

反应物

3
结构：COC(=O)c1cc(Cl)nc(Cl)c1
HCID93237

Methyl 2,6-dichloroisonicotinate

C7H5Cl2NO2

结构：CNS(C)(=O)=O
HCID97632

Methanesulfonamide, N-methyl-

C2H7NO2S

结构：CN(c1cc(C(=O)O)cc(Cl)n1)S(C)(=O)=O
HCID16748325

未命名化合物

PRODUCTS

生成物

1
结构：CC1CC1CN(C)c1cc(C(=O)O)cc(N(C)S(C)(=O)=O)n1
HCID59028283

未命名化合物

PROCEDURE

实验过程

Prepared from Methyl 2,6-dichloroisonicotinate, methyl(methylsulfonyl)amine and intermediate 3.3.1 following a similar procedure as described for the preparation of intermediate 4.2c.1. 1H NMR (400 MHz, CD3OD) δ 7.02 (s, 1H), 6.96 (s, 1H), 3.55 (A of ABX, dd, J=14.4, 6.0 Hz, 1H), 3.29 (B of ABX, dd, J=14.4, 7.2 Hz, 1H), 3.35 (s, 3H), 3.15 (s, 3H), 3.12 (s, 3H), 1.03 (d, J=6.0 Hz, 3H), 0.82-0.66 (m, 2H), 0.48-0.41 (m, 1H), 0.28-0.22 (m, 1H).