HCID 58505051, compound → HCID 58505108, compound

Participants

Reaction Steps

A suspension of Pd/C (10% w/w, 15 mg) and Intermediate 107 (0.25 g, 0.31 mmol) in MeOH (4 mL) was stirred under a balloon of hydrogen gas for 30 minutes, followed by filtration of the mixture through a pad of Celite diatomaceous earth, and concentration under reduced pressure. The title compound was provided as a white foam (0.13 g, 54%). ES/MS calcd. for C43H68N3O8Si+ 782.5. Found m/z=782.6 (M+H)+.

Provenance & Evidence