HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[2-[(6-Bromohexyl)oxy]ethyl]-4-nitrobenzene → (R)-8-hydroxy-5-(2,2,3,3-tetramethyl-16-(4-nitrophenyl)-4,14-dioxa-7-aza-3-silahexadecan-5-yl)quinolin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[2-[(6-Bromohexyl)oxy]ethyl]-4-nitrobenzene | HCID 13592784 | — |
| Reactant | (R)-8-hydroxy-5-(2,2,3,3-tetramethyl-18-(4-nitrophenyl)-4,14-dioxa-7-aza-3-silaoctadecan-5-yl)quinolin-2(1H)-one | HCID 58505188 | — |
| Product | (R)-8-hydroxy-5-(2,2,3,3-tetramethyl-16-(4-nitrophenyl)-4,14-dioxa-7-aza-3-silahexadecan-5-yl)quinolin-2(1H)-one | HCID 58505219 | — |
Reaction Steps
The title compound was synthesized in a manner analogous to that described for Intermediate 106, using Intermediate 53 in place of Intermediate 52. ES/MS calcd. for C31H46N3O6Si+ 584.3. Found m/z=584.4 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394829B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-b67de987fe1f4c61ad46c14e1d3a1d20 |
| Source note | uspto-grants-2013_03 |