HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 59350852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Benzene, 1-(ethylthio)-3-methyl- | HCID 141922 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 59350852 | HCID 59350852 | — |
Reaction Steps
Bromine (2.2 ml) was added to a solution of 1-(ethylthio)-3-methylbenzene (6.6 g) in acetic acid (20 ml) at 0° C. The mixture was stirred at RT for 2 h then the solvent removed under reduced pressure. The residue was purified by chromatography on silica eluting with DCM. Yield 6.6 g
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394986B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-206ccd3d7dc44eb7be592aa4a6634e44 |
| Source note | uspto-grants-2013_03 |