HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66995601, compound → HCID 66995497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66995601 | HCID 66995601 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66995497 | HCID 66995497 | — |
Reaction Steps
A mixture of the product from step (iii) (0.225 g), 10% palladium on carbon (0.05 g) in ethanol (20 ml) was hydrogenated at 1 Bar for 45 min. After filtration the solvent was evaporated under reduced pressure. Yield 0.22 g
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394986B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-f0509ee8eeb94fe0b15ec3ce14c128c1 |
| Source note | uspto-grants-2013_03 |