HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66995601, compound → HCID 66995959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66995601 | HCID 66995601 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66995959 | HCID 66995959 | — |
Reaction Steps
A mixture of the product from example 3 step (iii) (0.225 g), 10% palladium on carbon (0.05 g) and acetic acid (2 drops) in ethanol (20 ml) was hydrogenated at 3 Bar for 2 h then SBar for 5 h. After filtration the solvent was evaporated under reduced pressure. Yield 0.16 g
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394986B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-7e44ec4f35cc4eaab60ac876f36788be |
| Source note | uspto-grants-2013_03 |