Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Lithium Chloride | HCID 433294 | — |
| Reactant | HCID 86034419 | HCID 86034419 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 66995735 | HCID 66995735 | — |
Reaction Steps
A mixture of the product from step (ii) (0.75 g) and lithium chloride (0.345 g) in DMF (20 ml) was heated at 150° C. for 6 h, cooled and partitioned between ethylacetate/2M hydrochloric acid. The organics were dried and evaporated under reduced pressure, yield 0.7 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08394986B2 |
|---|
| Source dataset | uspto-grants-2013_03 |
|---|
| ORD ID | ord-af4b834a179b4de5a80f6345d4ef3f5e |
|---|
| Source note | uspto-grants-2013_03 |
|---|
