HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66995743, compound → HCID 66995495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66995743 | HCID 66995743 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 66995495 | HCID 66995495 | — |
Reaction Steps
A mixture of the product from step (ii) (1.4 g) and 10% Pd/C (0.14 g) in ethylacetate (30 ml) was hydrogenated at 2 Bar for 3 h then filtered through celite. The filtrate was evaporated under reduced pressure, yield 0.6 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394986B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-7598a5b132ae4793ba6b217f19d2831d |
| Source note | uspto-grants-2013_03 |