참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nonan-5-ol | HCID 12202 | — |
| 반응물 | 2-iodobenzenesulfonic Acid | HCID 2778247 | — |
| 반응물 | Potassium hydroxy sulfite | HCID 23707502 | — |
| 용매 | Nitromethane | HCID 6375 | — |
| 생성물 | 5-Nonanone | HCID 10405 | — |
반응 단계
1.7 mg (0.006 mmol) of 2-iodobenzenesulfonic acid, prepared by Preparation Example 1, 1.11 g (1.8 mmol) of powdered Oxone (registered trademark) and 433 mg (3 mmol) of 5-nonanol were added to 3.75 ml of nitromethane, and the mixture was heated at 70° C. while being stirred for 7.5 hours. The later treatment was carried out in the same way as in Example 1, and then 5-nonanone was obtained. The yield of the obtained 5-nonanone was determined and the result is shown in Table 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08394995B2 |
|---|
| 출처 데이터셋 | uspto-grants-2013_03 |
|---|
| ORD ID | ord-ee37b432431a48e68c72e42bbe0dc518 |
|---|
| 출처 메모 | uspto-grants-2013_03 |
|---|
