反应详情

A solution of Intermediate 63 (1.9 g) in methanol (400 mL) was hydrogenated using the H-Cube (settings: room temp, 1.3 ml/min flow rate) and 10% Pd/C CatCart 30 as the catalyst. The solvent was concentrated under vacuum to give the title compound (1.7 g). LC/MS MH+ 207 Rt 0.75 min (5 minute run).

1. concentrationThe solvent was concentrated under vacuum