HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 86668503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 68153467 | HCID 68153467 | — |
| Product | HCID 86668503 | HCID 86668503 | 98% |
Reaction Steps
In close analogy to the procedure described for the preparation of Intermediate XVIII-1, the reaction of 5-[3-(6-chloro-1H-benzoimidazol-2-yl)-phenyl]-5-methyl-morpholin-3-one (202 mg, 0.6 mmol) with Lawesson's reagent yielded the title compound (210 mg, 98% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399459B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-5189c7acd8bd4355af1c9956b6eef279 |
| Source note | uspto-grants-2013_03 |