HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 86668504, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 68153442 | HCID 68153442 | — |
| Product | HCID 86668504 | HCID 86668504 | 57% |
Reaction Steps
In close analogy to the procedure described for the preparation of Intermediate XVIII-1, the reaction of (RS)-5-[3-(5-chloro-benzooxazol-2-yl)-phenyl]-5-methyl-morpholin-3-one with Lawesson's reagent yielded the title compound (57% of theory). MS (ISP): m/z=359.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399459B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-b052a0404b1b436d936db0f03bc2d8ed |
| Source note | uspto-grants-2013_03 |