HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178478138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59742752 | HCID 59742752 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178478138 | HCID 178478138 | 100% |
Reaction Steps
Benzyl-(1-trityl-1H-imidazol-4-yl)-amine (0.15 g, 0.35 mmol) was dissolved in a 4 M solution of HCl in dioxane (5 ml). The mixture was stirred at room temperature for 90 minutes and then concentrated in vacuo. The residue was triturated in ether to yield the title compound as an off-white solid (73 mg, 100%); MS (ISP): 174.4 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399463B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-de44f4eb61874aa3922103312d467725 |
| Source note | uspto-grants-2013_03 |