HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178458730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 59829873 | HCID 59829873 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178458730 | HCID 178458730 | 122.7% |
Reaction Steps
Crude 2,4-bis-allyloxy 5-(but-2-ynyl)-N-[4-(morpholin-4-ylmethyl)-phenyl]-thiobenzamide (F470-IM10: 240 mg, 0.86 mmol) and hydrazine monohydrate (700 mg, 14 mmol) were dissolved in ethanol (6 mL) and the mixture was heated under reflux for 1 hour and then concentrated to obtain the crude title compound (F470-IM11: 243 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399464B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-8c64933088bb40b187438f0afcd5aba7 |
| Source note | uspto-grants-2013_03 |