Lawesson's reagent → HCID 59829845, compound

Participants

Reaction Steps

2,4-bis-benzyloxy-5-isopropyl-N-piperidin-1-yl-benzamide (F67-02: 198 mg, 0.43 mmol), toluene (5 mL) and Lawesson's reagent (157 mg, added in two portions) were placed in a test tube and heated for 2.5 hours under reflux. After the reaction was completed, the reaction mixture was concentrated under reduced pressure. The foam thus obtained was subjected to the next reaction without further purification.

Provenance & Evidence