HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → Diethyl(4-amino-3-methoxybenzyl)phosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | Ethyl(4-amino-3-methoxybenzyl)methylphosphinate | HCID 86653998 | — |
| Product | Diethyl(4-amino-3-methoxybenzyl)phosphonate | HCID 86653997 | — |
Reaction Steps
This material was prepared according to the procedure described above for ethyl(4-amino-3-methoxybenzyl)methylphosphinate using triethylphosphite in the first step. MS (ES+): m/z 274.01 [MH+] (ZQ3, polar 5 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399433B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-15752ec06e8c444891901f37631ed3e4 |
| Source note | uspto-grants-2013_03 |