反应详情

The title compound was prepared according to the procedure for Compound 102B (5-fluoro-N-methyl-2-nitrobenzamide) using 2-fluoro-6-nitrobenzoic acid. 1H NMR (CDCl3, 400 MHz): δ=3.09 (d, J=5.05 Hz, 3H), 7.45 (td, J=8.34, 1.01 Hz, 1H), 7.56 (td, J=8.27, 5.43 Hz, 1H), 7.94 (dt, J=8.08, 1.01 Hz, 1H). MS (ES+): m/z 199.05 [MH+] (TOF, polar).