HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-6-nitrobenzoic acid → 2-fluoro-N-methyl-6-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-6-nitrobenzoic acid | HCID 603758 | — |
| Reactant | 5-Fluoro-N-methyl-2-nitrobenzamide | HCID 44203077 | — |
| Product | 2-fluoro-N-methyl-6-nitrobenzamide | HCID 67255708 | — |
Reaction Steps
The title compound was prepared according to the procedure for Compound 102B (5-fluoro-N-methyl-2-nitrobenzamide) using 2-fluoro-6-nitrobenzoic acid. 1H NMR (CDCl3, 400 MHz): δ=3.09 (d, J=5.05 Hz, 3H), 7.45 (td, J=8.34, 1.01 Hz, 1H), 7.56 (td, J=8.27, 5.43 Hz, 1H), 7.94 (dt, J=8.08, 1.01 Hz, 1H). MS (ES+): m/z 199.05 [MH+] (TOF, polar).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399433B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-8c5e58d56a154b40a9a2baae50b09bec |
| Source note | uspto-grants-2013_03 |