Hydrochloric Acid → HCID 12595641, compound

HRID 1948605Notes

Reaction equation

HRID 1948605 reaction equation
Cl.[CH3:2][N:3]([CH3:21])[C:4]1([C:14]2[CH:15]=[C:16]([CH3:20])[CH:17]=[CH:18][CH:19]=2)[CH2:13][CH2:12][C:7]2(OCC[O:8]2)[CH2:6][CH2:5]1.Cl>O>[CH3:2][N:3]([CH3:21])[C:4]1([C:14]2[CH:15]=[C:16]([CH3:20])[CH:17]=[CH:18][CH:19]=2)[CH2:13][CH2:12][C:7](=[O:8])[CH2:6][CH2:5]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 68976332HCID 68976332, compound

Product 1

HCID 12595641HCID 12595641, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Dimethyl-(8-m-tolyl-1,4-dioxa-spiro[4.5]dec-8-yl)-amine hydrochloride (2.76 g, 10 mmole) was dissolved in water (4.2 ml), conc. hydrochloric acid (6.15 ml) was added and the mixture was stirred for 76 hours at RT.

Sources & evidence

ORD record
ord-33506e1d09344ca4adba582ba4346741
Source dataset
uspto-grants-2013_03
Patent number
US08399503B2

Reaction notes

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