HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile--water (1/1) → HCID 58277330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile--water (1/1) | HCID 18373917 | — |
| Reactant | HCID 58277295 | HCID 58277295 | — |
| Reactant | HCID 58277326 | HCID 58277326 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 58277330 | HCID 58277330 | — |
Reaction Steps
The preparation of the title compound takes place starting from the compound of Example 69A in analogy to the synthesis of the compound of Example 71A and with purification by preparative HPLC (RP18 column; mobile phase: acetonitrile/water gradient with the addition of 0.1% formic acid). 46 mg (100% of theory) of the title compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399682B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-e6165780e3334aa8816aba2d1793a346 |
| Source note | uspto-grants-2013_03 |