HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 58277440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 58277419 | HCID 58277419 | — |
| Reactant | HCID 67153505 | HCID 67153505 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 58277440 | HCID 58277440 | — |
Reaction Steps
The preparation of the title compound takes place starting from the compound of Example 119A and pyrrolidine without the addition of 0.1% formic acid in the preparative HPLC in analogy to the synthesis of the compound of Example 29. 2.5 mg (5% of theory) of the title compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399682B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-7149d74b6aa341a7beabdc3dc2f94ba0 |
| Source note | uspto-grants-2013_03 |